{"id":233,"date":"2024-01-10T09:24:52","date_gmt":"2024-01-10T01:24:52","guid":{"rendered":"https:\/\/shandong.nugene.com.cn\/?p=233"},"modified":"2024-01-10T09:24:53","modified_gmt":"2024-01-10T01:24:53","slug":"hplc%e6%b5%8b%e5%ae%9a%e6%b0%a8%e7%b3%96%e8%bd%af%e9%aa%a8%e7%b4%a0%e5%a5%b6%e7%b2%89%e4%b8%ad%e7%a1%ab%e9%85%b8%e8%bd%af%e9%aa%a8%e7%b4%a0","status":"publish","type":"post","link":"https:\/\/shandong.nugene.com.cn\/index.php\/hplc%e6%b5%8b%e5%ae%9a%e6%b0%a8%e7%b3%96%e8%bd%af%e9%aa%a8%e7%b4%a0%e5%a5%b6%e7%b2%89%e4%b8%ad%e7%a1%ab%e9%85%b8%e8%bd%af%e9%aa%a8%e7%b4%a0\/","title":{"rendered":"HPLC\u6d4b\u5b9a\u6c28\u7cd6\u8f6f\u9aa8\u7d20\u5976\u7c89\u4e2d\u786b\u9178\u8f6f\u9aa8\u7d20"},"content":{"rendered":"\n<p>\u9ad8\u6653\u96ea*\uff0c\u738b\u521a\uff0c\u5bab\u5efa\u8f89\uff0c\u590f\u65b0\u6708\uff0c\u8463\u5f66\u535a<\/p>\n\n\n\n<p>\u5317\u4eac\u59ff\u7f8e\u5802\u751f\u7269\u6280\u672f\u80a1\u4efd\u6709\u9650\u516c\u53f8\uff08\u5317\u4eac 100144\uff09<\/p>\n\n\n\n<p><strong>\u6458 \u8981<\/strong> \u4e3a\u5efa\u7acb\u9002\u5408\u6c28\u7cd6\u8f6f\u9aa8\u7d20\u5976\u7c89\u4e2d\u6d4b\u5b9a\u786b\u9178\u8f6f\u9aa8\u7d20\u7684\u65b9\u6cd5, \u6839\u636e\u4fdd\u5065\u98df\u54c1\u6cd5\u89c4\u3001\u56fd\u5bb6\u6807\u51c6\u53ca\u4ea7\u54c1\u539f\u8f85\u6599\u7ec4\u6210\u786e\u5b9a\u8be5\u4ea7\u54c1\u4e2d\u786b\u9178\u8f6f\u9aa8\u7d20\u7684\u6d4b\u5b9a\u65b9\u6cd5\u3002\u4ee5\u620a\u70f7\u78fa\u9178\u94a0\u6eb6\u6db2\u4e3a\u6d41\u52a8\u76f8A, \u4e59\u8148\u4e3a\u6d41\u52a8\u76f8B, \u68af\u5ea6\u6d17\u8131, Nncleodur C18 (\u7528\u6781\u6027\u5c0f\u5206\u5b50\u5c01\u5c3e, 250 mm\u00d74.6 mm, 5 \u03bcm) \u4e3a\u8272\u8c31\u67f1, \u8fdb\u6837\u91cf10 \u03bcL, \u6d41\u901f0.8 m L\/min, \u5728192 nm\u6ce2\u957f\u4e0b\u5bf9\u6c28\u7cd6\u8f6f\u9aa8\u7d20\u5976\u7c89\u4e2d\u786b\u9178\u8f6f\u9aa8\u7d20\u542b\u91cf\u8fdb\u884c\u68c0\u6d4b\u3002\u7ed3\u679c\u8868\u660e: \u786b\u9178\u8f6f\u9aa8\u7d20\u5728100.29~1 002.9 \u03bcg\/m L\u8303\u56f4\u5185\u4e0e\u5cf0\u9762\u79ef\u5448\u826f\u597d\u7684\u7ebf\u6027\u5173\u7cfb, R2=0.999 6; \u786b\u9178\u8f6f\u9aa8\u7d20\u68c0\u51fa\u9650\u548c\u5b9a\u91cf\u9650\u5206\u522b\u4e3a1.50 \u03bcg\/m L\u548c16.23 \u03bcg\/m L, 3\u4e2a\u6d53\u5ea6\u6c34\u5e73\u7684\u52a0\u6807\u56de\u6536\u7387\u4e3a99.95% (SRSD=2.76%)\u30026\u6279\u6837\u54c1\u4e2d, \u786b\u9178\u8f6f\u9aa8\u7d20\u542b\u91cf\u4e3a1.91~2.05 g\/100 g\u3002\u8be5\u65b9\u6cd5\u64cd\u4f5c\u7b80\u5355\u3001\u7ebf\u6027\u5173\u7cfb\u597d\u3001\u51c6\u786e\u5ea6\u9ad8\u3001\u7cbe\u5bc6\u5ea6\u3001\u56de\u6536\u7387\u7b49\u826f\u597d, \u53ef\u7528\u4e8e\u6c28\u7cd6\u8f6f\u9aa8\u7d20\u5976\u7c89\u4e2d\u786b\u9178\u8f6f\u9aa8\u7d20\u7684\u8d28\u91cf\u63a7\u5236\u3002<\/p>\n\n\n\n<p><strong>\u5173\u952e\u8bcd<\/strong> <strong>\u786b\u9178\u8f6f\u9aa8\u7d20; \u6c28\u7cd6\u8f6f\u9aa8\u7d20\u5976\u7c89; \u6d4b\u5b9a\u65b9\u6cd5<\/strong><\/p>\n\n\n\n<p>Determination of Chondroitin Sulfate in Aminochondroitin Milk Powder by HPLC<\/p>\n\n\n\n<p>GAO Xiaoxue*, WANG Gang, GONG Jianhui, XIA Xinyue, DONG Yanbo<\/p>\n\n\n\n<p>Beijing Zimeitang Biotechnology Corporation (Beijing 100144)<\/p>\n\n\n\n<p><strong>Abstract<\/strong>\u3000 In order to establish a suitable method for the determination of chondroitin sulfate in aminochondroitin milk powder, the determination method of chondroitin sulfate in the product was determined according to health food regulations, national standards and the composition of raw materials. Sodium pentanesulfonic acid solution was used as mobile phase A, acetonitrile as mobile phase B, gradient elution, Nncleodur C18 (tail sealed with polar small molecules, 250 mm\u00d74.6 mm, 5 um) was used as the chromatographic column, the sample size was 10 \u03bcL, and the \ufb01ow rate was 0.8 m L\/min. The content of chondroitin sulfate in ammoniated chondroitin milk powder was detected at 192 nm wavelength. The results showed that chondroitin sulfate had a good linear relationship with peak area in the range of 100.29-1 002.9 \u03bcg\/m L, R2=0.999 6; The limits of detection and quantifcation of chondroitin sulfate were 1.50 \u03bcg\/m L and 16.23 \u03bcg\/m L, respectively. The recoveries of the three concentrations were 99.95% (SRSD=2.76%). The contents of chondroitin sulfate in 6 batches of samples ranged from 1.91 g\/100 g to 2.05 g\/100 g. The method had the advantages of simple operation, good linear relationship, high accuracy, precision and good recovery rate. It could be used for the quality control of chondroitin sulfate in aminochondroitin milk powder.<\/p>\n\n\n\n<p><strong>Keywords\u3000 chondroitin sulfate; gummy chondroitin collagen calcium milk powder; determination method<\/strong><\/p>\n\n\n\n<p>\u786b\u9178\u8f6f\u9aa8\u7d20\uff08chondroitiulfate\uff0cCS\uff09\u4f5c\u4e3a\u4e00\u79cd\u5177\u6709\u5929\u7136\u6d3b\u6027\u7684\u9178\u6027\u9ecf\u591a\u7cd6\u7c7b\u7269\u8d28\uff0c\u5176\u5e7f\u6cdb\u5b58\u5728\u4e8e\u52a8\u7269\u7684\u8f6f\u9aa8\u548c\u7ed3\u7f14\u7ec4\u7ec7\u4e2d[1]\u3002\u5728\u4e34\u5e8a\u5e94\u7528\u5f53\u4e2d\u5176\u5177\u6709\u8c03\u8282\u8840\u8102\u3001\u6297\u80bf\u7624\u3001\u6297\u8870\u8001\u3001\u6cbb\u7597\u5173\u8282\u708e\u3001\u9632\u6cbb\u51a0\u5fc3\u75c5\u7b49\u591a\u79cd\u7597\u6548\uff0c\u5e76\u4e14\u4e0d\u826f\u53cd\u5e94\u5c11[2-5]\u3002\u6b64\u5916\uff0c\u786b\u9178\u8f6f\u9aa8\u7d20\u88ab\u5e7f\u6cdb\u5e94\u7528\u4e8e\u98df\u54c1\u53ca\u5316\u5986\u54c1\u4e2d\uff0c\u8fd8\u5177\u6709\u6539\u5584\u53e3\u611f\u3001\u6da6\u6ed1\u5ea6\u3001\u5438\u6e7f\u6027\u7b49\u4f5c\u7528[2-7]\u3002\u56e0\u6b64\uff0c\u6d4b\u5b9aCS\u542b\u91cf\u7684\u5206\u6790\u65b9\u6cd5\u5bf9\u4e8e\u4fdd\u5065\u98df\u54c1\u548c\u836f\u54c1\u539f\u6599\u53ca\u6210\u54c1\u9500\u552e\u7684\u54c1\u8d28\u63a7\u5236\u975e\u5e38\u91cd\u8981\u3002<\/p>\n\n\n\n<p>\u786b\u9178\u8f6f\u9aa8\u7d20\u662f\u7531D-\u8461\u7cd6\u919b\u9178\u548cN-\u4e59\u9170\u6c28\u57fa\u534a\u4e73\u7cd6\u4ee5\u03b2-1, 4-\u7cd6\u82f7\u952e\u8fde\u63a5\u800c\u6210\u7684\u91cd\u590d\u4e8c\u7cd6\u5355\u4f4d\u7ec4\u6210\u7684\u591a\u7cd6\u3002\u6d4b\u5b9aCS\u542b\u91cf\u7684\u5e38\u7528\u65b9\u6cd5\u6709\u5206\u5149\u5149\u5ea6\u6cd5\u3001\u9ad8\u6548\u6db2\u76f8\u6cd5\u548c\u7535\u5316\u5b66\u5206\u6790\u6cd5\u7b49[1-6]\u3002\u5206\u5149\u5149\u5ea6\u6cd5\u4e3b\u8981\u662f\u901a\u8fc7\u5229\u7528\u5206\u5149\u5149\u5ea6\u4eea\u6d4b\u5b9a\u4e8c\u7cd6\u5728\u7279\u5b9a\u6761\u4ef6\u4e0b\u4e0e\u8bd5\u5242\u53cd\u5e94\u751f\u6210\u6709\u8272\u7269\u8d28\u6216\u6c89\u6dc0\u3002\u4f46\u7531\u4e8e\u7cd6\u80fa\u805a\u7cd6\u7684\u7ed3\u6784\u76f8\u4f3c\u5ea6\u9ad8\uff0c\u4e14\u8f6f\u9aa8\u4e2d\u5bcc\u542b\u591a\u79cd\u9ecf\u591a\u7cd6\uff0c\u5e72\u6270\u56e0\u7d20\u591a\uff0c\u90a3\u4e48\u91cd\u73b0\u6027\u5dee\uff0c\u800c\u4e14\u8be5\u65b9\u6cd5\u9700\u8981\u4f7f\u7528\u6bd2\u6027\u8f83\u5f3a\u7684\u8bd5\u5242\uff0c\u5b58\u5728\u6f5c\u5728\u5371\u5bb3[2, 4]\u3002\u7535\u5316\u5b66\u5206\u6790\u6cd5\u5bf9\u64cd\u4f5c\u4eba\u5458\u8bd5\u9a8c\u7d20\u8d28\u8981\u6c42\u9ad8\uff0c\u4e14\u8bd5\u9a8c\u6761\u4ef6\u8981\u6c42\u4e25\u683c\uff0c\u4e13\u5c5e\u6027\u6bd4\u8f83\u5f3a[6]\u3002\u9ad8\u6548\u6db2\u76f8\u6cd5\u4e3b\u8981\u662f\u5c06\u591a\u7cd6\u5206\u89e3\u540e\u8fdb\u5165\u8272\u8c31\u67f1\u5229\u7528\u5404\u7ec4\u5206\u95f4\u6781\u6027\u5dee\u5f02\u7684\u6027\u8d28\u8fdb\u884c\u5206\u79bb\u540e\u68c0\u6d4b\uff0c\u8be5\u65b9\u6cd5\u6d4b\u5b9a\u5bf9\u8c61\u5355\u4e00\uff0c\u65e0\u6742\u8d28\u5e72\u6270\uff0c\u7075\u654f\u5ea6\u9ad8\uff0c\u9002\u7528\u6027\u5e7f\u3002\u5df2\u6709\u7684GB\/T 20365\u20142006\u300a\u786b\u9178\u8f6f\u9aa8\u7d20\u548c\u76d0\u9178\u6c28\u57fa\u8461\u8404\u7cd6\u542b\u91cf\u7684\u6d4b\u5b9a \u6db2\u76f8\u8272\u8c31\u6cd5\u300b\u662f\u901a\u8fc7\u7528\u6db2\u76f8\u8272\u8c31\u6d4b\u5b9a\u786b\u9178\u8f6f\u9aa8\u7d20\u7684\u65b9\u6cd5[2-3, 7-9]\u3002<\/p>\n\n\n\n<p>\u8bd5\u9a8c\u6d4b\u8bd5\u54c1\u9009\u62e9\u6c28\u7cd6\u8f6f\u9aa8\u7d20\u5976\u7c89\uff0c\u542b\u6709\u5927\u91cfCS\uff0c\u9664\u6b64\u4e4b\u5916\u8fd8\u542b\u6709\u5176\u4ed6\u98df\u54c1\u6210\u5206\uff0c\u5bf9\u6d4b\u5b9a\u4f1a\u6709\u8f83\u5927\u5e72\u6270\u3002\u56e0\u6b64\uff0c\u6709\u5fc5\u8981\u5efa\u7acb\u53ef\u5feb\u901f\u51c6\u786e\u6d4b\u5b9a\u6c28\u7cd6\u8f6f\u9aa8\u7d20\u5976\u7c89\u4e2d\u786b\u9178\u8f6f\u9aa8\u7d20\u542b\u91cf\u7684\u65b9\u6cd5\u3002\u8bd5\u9a8c\u4ee5\u6c28\u7cd6\u8f6f\u9aa8\u7d20\u5976\u7c89\u4e3a\u6d4b\u8bd5\u54c1\uff0c\u5229\u7528\u9ad8\u6548\u6db2\u76f8\u8272\u8c31\u4eea\uff0c\u901a\u8fc7\u4f18\u5316\u63d0\u53d6\u65b9\u6cd5\u3001\u6d41\u52a8\u76f8\u6d41\u901f\u7b49\u8272\u8c31\u6761\u4ef6\u5efa\u7acb\u540c\u65f6\u6d4b\u5b9a\u6c28\u7cd6\u8f6f\u9aa8\u7d20\u5976\u7c89\u4e2dCS\u542b\u91cf\u7684\u65b9\u6cd5\uff0c\u5e76\u5b8c\u6210\u65b9\u6cd5\u5b66\u9a8c\u8bc1\uff0c\u4ee5\u671f\u66f4\u597d\u5730\u7528\u4e8e\u6c28\u7cd6\u8f6f\u9aa8\u7d20\u5976\u7c89\u7684\u8d28\u91cf\u63a7\u5236\u3002<\/p>\n\n\n\n<p><strong>1\u3000\u4eea\u5668\u4e0e\u8bd5\u5242<\/strong><\/p>\n\n\n\n<p><strong>1.1\u3000\u4eea\u5668\u4e0e\u8bbe\u5907<\/strong><\/p>\n\n\n\n<p>\u9ad8\u6548\u6db2\u76f8\u8272\u8c31\u4eea[\u5c9b\u6d25\u4eea\u5668\uff08\u82cf\u5dde\uff09\u6709\u9650\u516c\u53f8]\uff1b\u7535\u5b50\u5929\u5e73\uff08d=0.01 mg\uff0c\u682a\u5f0f\u4f1a\u793e\u5c9b\u6d25\u5236\u4f5c\u6240\u65e5\u672c\u4eac\u90fd\uff09\uff1b\u7535\u5b50\u5929\u5e73[d=0.1 mg\uff0c\u8d5b\u591a\u5229\u65af\u79d1\u5b66\u4eea\u5668\uff08\u5317\u4eac\uff09\u6709\u9650\u516c\u53f8]\u3002<\/p>\n\n\n\n<p><strong>1.2\u3000\u6750\u6599\u4e0e\u8bd5\u5242<\/strong><\/p>\n\n\n\n<p>\u786b\u9178\u8f6f\u9aa8\u7d20\u94a0\uff08\u6279\u53f7140792-202003\uff0c\u4e2d\u56fd\u98df\u54c1\u836f\u54c1\u68c0\u5b9a\u7814\u7a76\u9662\uff09\uff1bD-\u76d0\u9178\u6c28\u57fa\u8461\u8404\u7cd6\uff08\u6279\u53f7140649-201606\uff0c\u4e2d\u56fd\u98df\u54c1\u836f\u54c1\u68c0\u5b9a\u7814\u7a76\u9662\uff09\uff1b\u65e0\u6c34\u4e59\u9187\uff08\u6279\u53f720201109\uff0c\u5929\u6d25\u5e02\u6d25\u4e1c\u5929\u6b63\u7cbe\u7ec6\u5316\u5b66\u8bd5\u5242\u5382\uff09\uff1b\u620a\u70f7\u78fa\u9178\u94a0\uff08\u6279\u53f720180761\uff0cMREDA\uff09\uff1b\u4e59\u8148\uff08\u6279\u53f7021902\uff0cMREDA\uff09\uff1b\u6c2f\u5316\u94a0\uff08\u6279\u53f720190818\uff0c\u5317\u4eac\u5e02\u7ea2\u661f\u5316\u5de5\u5382\uff09\uff1b\u4e2d\u6027\u6c27\u5316\u9176\uff08\u6279\u53f7515E011\uff0cSolarbio\uff09\uff1b\u78f7\u9178\u4e8c\u6c22\u94be\uff08\u6279\u53f720180117\uff0c\u5317\u4eac\u5316\u5de5\u5382\uff09\uff1b\u6c22\u6c27\u5316\u94a0\uff08\u6279\u53f720170104\uff0c\u5317\u4eac\u5316\u5de5\u5382\uff09\uff1b\u6c28\u7cd6\u8f6f\u9aa8\u7d20\u5976\u7c89\uff08\u6279\u53f720220101\uff0c\u5317\u4eac\u59ff\u7f8e\u5802\u751f\u7269\u6280\u672f\u80a1\u4efd\u6709\u9650\u516c\u53f8\uff09\u3002<\/p>\n\n\n\n<p><strong>2\u3000\u65b9\u6cd5\u4e0e\u7ed3\u679c<\/strong><\/p>\n\n\n\n<p><strong>2.1\u3000\u8272\u8c31\u6761\u4ef6<\/strong><\/p>\n\n\n\n<p>\u8272\u8c31\u67f1\u4e3aNncleodur C18\uff08\u7528\u6781\u6027\u5c0f\u5206\u5b50\u5c01\u5c3e\uff0c250 mm\u00d74.6 mm\uff0c5 \u03bcm\uff09\uff0c\u6d41\u52a8\u76f8A\u4e3a\u620a\u70f7\u78fa\u9178\u94a0\u6eb6\u6db2\uff0c\u6d41\u52a8\u76f8B\u4e3a\u4e59\u8148\u3002\u68af\u5ea6\u6d17\u8131\uff0c\u6d41\u901f0.8 m L\/min\uff0c\u67f1\u6e2935 \u2103\uff0c\u68c0\u6d4b\u6ce2\u957f192 nm\u65f6\uff0c\u8fdb\u6837\u91cf10 \u03bcL\u3002<\/p>\n\n\n\n<p><strong>2.1.1\u3000\u6d41\u52a8\u76f8\u4f18\u5316<\/strong><\/p>\n\n\n\n<p>\u4e3a\u6539\u5584\u5cf0\u5f62\u3001\u63d0\u9ad8\u6d4b\u5b9a\u7ed3\u679c\u7684\u51c6\u786e\u6027\u3001\u4fdd\u8bc1\u6210\u54c1\u8d28\u91cf\uff0c\u5bf9GB\/T 20365\u20142006\u300a\u786b\u9178\u8f6f\u9aa8\u7d20\u548c\u76d0\u9178\u6c28\u57fa\u8461\u8404\u7cd6\u542b\u91cf\u7684\u6d4b\u5b9a \u6db2\u76f8\u8272\u8c31\u6cd5\u300b\u89c4\u5b9a\u7684\u65b9\u6cd5\u4e2d\u7684\u8bd5\u6837\u6d41\u52a8\u76f8\u8fdb\u884c\u4f18\u5316\uff0c\u88681\u4e2d\u5e8f\u53f71\u7684\u6d41\u52a8\u76f8\u6bd4\u4f8b\u4e3a\u56fd\u6807\u89c4\u5b9a\u7684\u8272\u8c31\u76f8\u65b9\u6cd5\u3002\u7531\u88681\u548c\u56fe1\u53ef\u77e5\uff0c\u6839\u636e\u4e0d\u540c\u6d41\u52a8\u76f8\u8272\u8c31\u6761\u4ef6\u4e0b\u786b\u9178\u8f6f\u9aa8\u7d20\u5cf0\u5f62\u53ca\u5206\u79bb\u5ea6\uff0c\u786e\u5b9a\u6d41\u52a8\u76f8\u4e3a\u4e59\u8148+\u620a\u70f7\u78fa\u9178\u94a02+98\uff08V\/V\uff09\uff0c\u5176\u4ed6\u8272\u8c31\u6761\u4ef6\u4e0d\u53d8\u3002\u5728\u6b64\u6761\u4ef6\u4e0b\uff0c\u8272\u8c31\u5cf0\u5f62\u3001\u5206\u79bb\u5ea6\u4f1a\u6bd4\u8f83\u597d\u3002<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><img loading=\"lazy\" decoding=\"async\" width=\"367\" height=\"180\" src=\"https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-12.png\" alt=\"\" class=\"wp-image-234\" srcset=\"https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-12.png 367w, https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-12-300x147.png 300w\" sizes=\"auto, (max-width: 367px) 100vw, 367px\" \/><\/figure>\n\n\n\n<figure class=\"wp-block-image size-full\"><img loading=\"lazy\" decoding=\"async\" width=\"398\" height=\"330\" src=\"https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-13.png\" alt=\"\" class=\"wp-image-235\" srcset=\"https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-13.png 398w, https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-13-300x249.png 300w\" sizes=\"auto, (max-width: 398px) 100vw, 398px\" \/><\/figure>\n\n\n\n<figure class=\"wp-block-image size-full\"><img loading=\"lazy\" decoding=\"async\" width=\"379\" height=\"505\" src=\"https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-14.png\" alt=\"\" class=\"wp-image-236\" srcset=\"https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-14.png 379w, https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-14-225x300.png 225w\" sizes=\"auto, (max-width: 379px) 100vw, 379px\" \/><\/figure>\n\n\n\n<p><strong>2.2\u3000\u6eb6\u6db2\u7684\u5236\u5907<\/strong><\/p>\n\n\n\n<p><strong>2.2.1\u3000\u4f9b\u8bd5\u54c1\u6eb6\u6db2<\/strong><\/p>\n\n\n\n<p>\u5c065 mg\u6837\u54c1\u6eb6\u89e3\u572810 m L\u6c34\u4e2d\uff0c\u901a\u8fc7\u6c34\u8d85\u58f0\u63d0\u53d620 min\uff1b\u63d0\u53d6\u6db2\u4f7f\u7528\u5fae\u5b54\u6ee4\u819c\u630910 000 r\/min\u79bb\u5fc3\uff0c\u6447\u5300\uff0c\u6ee4\u8fc7\uff0c\u53d6\u7eed\u6ee4\u6db2\u3002<\/p>\n\n\n\n<p><strong>2.2.2\u3000\u5bf9\u7167\u54c1\u6eb6\u6db2\u5236\u5907<\/strong><\/p>\n\n\n\n<p>\u79f0\u53d625.48 mg\u786b\u9178\u8f6f\u9aa8\u7d20\u94a0\u5bf9\u7167\u54c1\u4e8e25 m L\u5bb9\u91cf\u74f6\u4e2d\uff0c\u52a0\u9002\u91cf\u6c34\u8d85\u58f0\u6eb6\u89e3\uff0c\u52a0\u6c34\u5b9a\u523b\u5ea6\uff0c\u4f5c\u4e3a\u5bf9\u7167\u54c1\u50a8\u5907\u6db2\u3002\u91cf\u53d65 m L\u5bf9\u7167\u54c1\u50a8\u5907\u6db2\u4e8e10 m L\u5bb9\u91cf\u74f6\u4e2d\uff0c\u52a0\u6c34\u5b9a\u5bb9\u81f3\u523b\u5ea6\uff0c\u4e3a\u5bf9\u7167\u54c1\u4f7f\u7528\u6db2\u3002<\/p>\n\n\n\n<p><strong>2.2.3\u3000\u9634\u6027\u5bf9\u7167\u6eb6\u6db2<\/strong><\/p>\n\n\n\n<p>\u6309\u4f9b\u8bd5\u54c1\u7684\u5904\u65b9\u5de5\u827a\u548c\u914d\u65b9\u6bd4\u4f8b\u5236\u5f97\u7f3a\u786b\u9178\u8f6f\u9aa8\u7d20\u7684\u9634\u6027\u6837\u54c1\u3002<\/p>\n\n\n\n<p><strong>2.3\u3000\u7ebf\u6027\u5173\u7cfb\u8003\u5bdf<\/strong><\/p>\n\n\n\n<p>\u79f0\u53d625.48 mg\u786b\u9178\u8f6f\u9aa8\u7d20\u5bf9\u7167\u54c1\uff0c\u6309\u71672.2.2\u7684\u65b9\u6cd5\u5236\u5907\u5bf9\u7167\u54c1\u50a8\u5907\u6db2\uff0c\u4f9d\u6b21\u91cf\u53d61\uff0c2\uff0c3\uff0c4\u548c5 m L\u5bf9\u7167\u54c1\u50a8\u5907\u6db2\u4e8e10 m L\u5bb9\u91cf\u74f6\u4e2d\uff0c\u52a0\u6c34\u5b9a\u5bb9\u81f3\u523b\u5ea6\uff0c\u4f5c\u4e3a\u5bf9\u7167\u54c1\u6807\u51c6\u5de5\u4f5c\u6db2\u6807\u51c6\u66f2\u7ebf\u3002\u6309\u7167\u8be5\u8bd5\u9a8c\u4f18\u5316\u597d\u7684\u6d41\u52a8\u76f8\u8272\u8c31\u6761\u4ef6\u65b9\u6cd5\u4e0b\u6d4b\u5b9a\uff0c\u7528\u5cf0\u9762\u79ef\uff08Y\uff09\u5bf9\u6d53\u5ea6\uff08X\uff09\u7ed8\u5236\u786b\u9178\u8f6f\u9aa8\u7d20\u7684\u6807\u51c6\u56de\u5f52\u66f2\u7ebf\u3002\u5982\u88682\u548c\u56fe2\u6240\u793a\u3002<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><img loading=\"lazy\" decoding=\"async\" width=\"369\" height=\"273\" src=\"https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-15.png\" alt=\"\" class=\"wp-image-237\" srcset=\"https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-15.png 369w, https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-15-300x222.png 300w\" sizes=\"auto, (max-width: 369px) 100vw, 369px\" \/><\/figure>\n\n\n\n<p><strong>2.4\u3000\u65b9\u6cd5\u5b66\u8003\u5bdf<\/strong><\/p>\n\n\n\n<p><strong>2.4.1\u3000\u7cbe\u5bc6\u5ea6\u8bd5\u9a8c<\/strong><\/p>\n\n\n\n<p>\u7cbe\u786e\u79f0\u53d6\u6837\u54c1\uff0c\u63092.2.2\u7684\u65b9\u6cd5\u5236\u5907\u4f9b\u8bd5\u54c1\uff0c\u63092.1.1\u7684\u4f18\u5316\u540e\u5f97\u8272\u8c31\u6761\u4ef6\u5e73\u884c\u6d4b\u5b9a6\u6b21\uff0c\u8ba1\u7b97\u7ed3\u679c\u786b\u9178\u8f6f\u9aa8\u7d20\u542b\u91cf\u3002\u88683\u6d4b\u5b9a\u7ed3\u679c\u8868\u660e\uff0c\u786b\u9178\u8f6f\u9aa8\u7d20\u7684\u5e73\u5747\u503c\uff08n=6\uff09\u5206\u522b\u4e3a2.03 g\/100g\uff0cSRSD\u4e3a0.81%\uff0c\u8868\u660e\u8be5\u6cd5\u7cbe\u5bc6\u5ea6\u826f\u597d\u3002<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><img loading=\"lazy\" decoding=\"async\" width=\"367\" height=\"186\" src=\"https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-16.png\" alt=\"\" class=\"wp-image-238\" srcset=\"https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-16.png 367w, https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-16-300x152.png 300w\" sizes=\"auto, (max-width: 367px) 100vw, 367px\" \/><\/figure>\n\n\n\n<p><strong>2.4.2\u3000\u7a33\u5b9a\u6027\u8bd5\u9a8c<\/strong><\/p>\n\n\n\n<p>\u53d6\u6837\u54c1\uff0c\u63092.2.1\u7684\u65b9\u6cd5\u5236\u5907\u4f9b\u8bd5\u54c1\u6eb6\u6db2\uff0c\u5ba4\u6e29\u653e\u7f6e0\uff0c2\uff0c4\uff0c6\uff0c8\uff0c10\u548c12 h\uff0c\u6309\u71672.1\u8272\u8c31\u6761\u4ef6\u6d4b\u5b9a\uff0c\u8bb0\u5f55\u786b\u9178\u8f6f\u9aa8\u7d20\u542b\u91cf\uff0cSRSD\u4e3a0.8%\uff0c\u8868\u660e\u8be5\u6cd5\u91cd\u590d\u6027\u826f\u597d\uff0c\u8868\u660e\u4f9b\u8bd5\u54c1\u6eb6\u6db2\u5728\u5ba4\u6e2912 h\u5185\u7a33\u5b9a\u6027\u826f\u597d\u3002<\/p>\n\n\n\n<p><strong>2.4.3\u3000\u91cd\u590d\u6027\u8bd5\u9a8c<\/strong><\/p>\n\n\n\n<p>\u53d6\u6837\u54c16\u4efd\uff0c\u5206\u522b\u63092.2.1\u7684\u65b9\u6cd5\u5236\u5907\u4f9b\u8bd5\u54c1\u6eb6\u6db2\uff0c\u6309\u71672.1\u7684\u8272\u8c31\u6761\u4ef6\u6d4b\u5b9a\uff0c\u786b\u9178\u8f6f\u9aa8\u7d20\u542b\u91cf1.98 g\/100 g\uff0cSRSD\u5206\u522b\u4e3a3.7%\u3002<\/p>\n\n\n\n<p><strong>2.4.4\u3000\u56de\u6536\u7387\u8bd5\u9a8c<\/strong><\/p>\n\n\n\n<p>\u5e73\u884c\u5206\u522b\u79f0\u53d66\u4efd\u7684\u6837\u54c1\uff0c\u5404\u52a0\u5165\u786b\u9178\u8f6f\u9aa8\u7d20\u94a0\u6807\u51c6\u54c1\uff08\u7eaf\u5ea698.4%\uff09\u7ea612.8 mg\uff0c\u52a0\u516525 m L\u6c34\uff0c\u8d85\u58f020 min\uff0c\u630910 000 r\/min\u79bb\u5fc310 min\uff0c\u53d61 m L\u4e0a\u5fae\u5b54\u6ee4\u819c\uff083 000\u9053\u5c14\u987f\uff09\uff0c\u630910 000 r\/min\u79bb\u5fc330 min\uff0c\u4e0b\u6e05\u6db2\u5f03\u53bb\uff1b\u5728\u5fae\u5b54\u6ee4\u819c\u4e0a\u52a0\u51652.0 m L\u6c34\uff0c\u630910 000 r\/min\u79bb\u5fc330 min\uff0c\u7cbe\u786e\u52a0\u51652.0 m L\u6c34\uff0c\u8d85\u58f05 min\uff0c\u53d6\u51fa\u8fc70.45 \u03bcm\u6ee4\u819c\u3002\u6309\u71672.1.1\u7684\u8272\u8c31\u6761\u4ef6\u8fdb\u884c\u6d4b\u5b9a\uff0c\u5e76\u8ba1\u7b97\u786b\u9178\u8f6f\u9aa8\u7d20\u7684\u52a0\u6837\u56de\u6536\u7387\uff0c\u7ed3\u679c\u89c1\u88684\u3002<\/p>\n\n\n\n<figure class=\"wp-block-image size-full is-resized\"><img loading=\"lazy\" decoding=\"async\" width=\"554\" height=\"120\" src=\"https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-17.png\" alt=\"\" class=\"wp-image-239\" style=\"width:554px;height:auto\" srcset=\"https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-17.png 554w, https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-17-300x65.png 300w\" sizes=\"auto, (max-width: 554px) 100vw, 554px\" \/><\/figure>\n\n\n\n<p><strong>2.4.5\u3000\u68c0\u51fa\u9650\u548c\u5b9a\u91cf\u9650<\/strong><\/p>\n\n\n\n<p>\u53d62.3\u7684\u6700\u4f4e\u6d53\u5ea6\u7684\u6df7\u5408\u5bf9\u7167\u54c1\u6eb6\u6db2\uff0c\u7528\u6c34\u9010\u6b65\u7a00\u91ca\u5e76\u8fdb\u884c\u6d4b\u5b9a\uff0c\u5206\u522b\u63092.1.1\u7684\u8272\u8c31\u6761\u4ef6\u8fdb\u884c\u6d4b\u5b9a\uff0c\u8bb0\u5f55\u4fe1\u53f7\u5f3a\u5ea6\u4e0e\u566a\u97f3\u5f3a\u5ea6\u7684\u6bd4\u503c\uff0c\u5c06\u4fe1\u53f7\u5f3a\u5ea6\u548c\u566a\u97f3\u5f3a\u5ea6\u4e4b\u6bd4\u7ea6\u4e3a3\u500d\u4fe1\u566a\u6bd4\u548c10\u500d\u4fe1\u566a\u6bd4\u4f5c\u4e3a\u68c0\u51fa\u9650\u548c\u5b9a\u91cf\u9650\uff0c\u786b\u9178\u8f6f\u9aa8\u7d20\u7684\u68c0\u51fa\u9650\u4e3a1.50 \u03bcg\/m L\uff0c\u5b9a\u91cf\u9650\u4e3a16.23 \u03bcg\/m L\u3002\u7ed3\u679c\u8868\u660e\uff0c\u8bd5\u9a8c\u65b9\u6cd5\u6d4b\u5f97\u7684\u65b9\u6cd5\u68c0\u51fa\u9650\u548c\u65b9\u6cd5\u5b9a\u91cf\u9650\u5747\u5c0f\u4e8e\u6807\u51c6\u89c4\u5b9a\u7684\u68c0\u51fa\u9650\u548c\u5b9a\u91cf\u9650\uff0c\u8bd5\u9a8c\u65b9\u6cd5\u6d4b\u5b9a\u786b\u9178\u8f6f\u9aa8\u7d20\u7684\u7075\u654f\u5ea6\u8f83\u9ad8\uff0c\u80fd\u591f\u6ee1\u8db3\u542b\u91cf\u6d4b\u5b9a\u7684\u9700\u8981\u3002<\/p>\n\n\n\n<p><strong>2.4.6\u3000\u6837\u54c1\u542b\u91cf\u6d4b\u5b9a<\/strong><\/p>\n\n\n\n<p>\u53d64\u6279\u6b21\u6837\u54c1\uff0c\u5206\u522b\u63092.2.1\u7684\u65b9\u6cd5\u5236\u5907\u4f9b\u8bd5\u54c1\u6eb6\u6db2\uff0c\u6bcf\u6279\u5e73\u884c3\u4efd\uff0c\u63092.1.1\u7684\u8272\u8c31\u6761\u4ef6\u6d4b\u5b9a\uff0c\u8bb0\u5f55\u5cf0\u9762\u79ef\uff0c\u6309\u5916\u6807\u6cd5\u8ba1\u7b97\u786b\u9178\u8f6f\u9aa8\u7d20\u542b\u91cf\uff0c\u7ed3\u679c\u89c1\u88685\u3002<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><img loading=\"lazy\" decoding=\"async\" width=\"371\" height=\"175\" src=\"https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-18.png\" alt=\"\" class=\"wp-image-240\" srcset=\"https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-18.png 371w, https:\/\/shandong.nugene.com.cn\/wp-content\/uploads\/2024\/01\/image-18-300x142.png 300w\" sizes=\"auto, (max-width: 371px) 100vw, 371px\" 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